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  1 saw   1.1 \documentclass{chowto}
  2           
  3           \title{Drift Chamber Gas System Operation}
  4           \howtotype{expert} % ``expert'', ``user'', ``reference''
  5           %\experiment{Name of experiment} % Optional
  6           \author{H. Fenker}
  7           \category{general} % Subject area of this document
  8           
  9 saw   1.5 \maintainer{H. Fenker} % Optional
 10           \date{December 18, 2007} % Can use \today as the argument
 11 saw   1.1 
 12 saw   1.5 %To attempt to make pretty-looking pdf files...(not standard howto)
 13           \usepackage[T1]{fontenc}
 14           \usepackage{pslatex}
 15 saw   1.1 
 16           \begin{document}
 17           \providecommand{\degg}{\ensuremath{^{\circ}\ }}
 18           
 19           \begin{abstract}
 20 saw   1.5 This document provides detailed setup information for the drift
 21           chamber gas mixing system, as well as the correct procedure for
 22           refilling the alcohol supply and changing gas bottles. This
 23           information is intended for use by {\bf gas system experts only.}  For
 24           day-to-day shift worker instructions, refer to the corresponding {\it
 25           user} howto document.
 26           
 27           {\bf Please Note:} The Hall-C Drift Chamber Gas System was
 28           significantly changed in early 2007. It is now a {\it pressure-driven
 29           system} whereas it had been flow-controlled. Long-time Hall-C staff
 30           and users will find that the system operates quite differently now.
 31 saw   1.1 \end{abstract}
 32           
 33 saw   1.5 %=====================================================================
 34           %=====================================================================
 35 saw   1.1 \section{Overview}
 36           
 37 saw   1.5 The drift chamber gas is composed of 50\% Argon and 50\% Ethane (by
 38           volume), bubbled through isopropanol maintained at a temperature such
 39           that the gas mixture contains approximately 1\% alcohol vapor. The
 40           mixing system that produces this gas is housed in the Hall-C gas shed
 41           (Bldg. 96c). The bottles supplying the gas to the mixing system are
 42           attached to two two-bottle manifolds outside the gas shed, within the
 43           fenced-in gas bottle yard.
 44           
 45           A single mixing system provides the gas for both the SOS and the HMS
 46           detectors. Gas is delivered to the hall at a pressure of about 9 psi
 47           (500~Torr) above atmospheric pressure.  Each detector's flow is
 48           controlled by its own individual needle-valve with flowmeter, located
 49           in the appropriate shield house, near the detector. The job of the
 50           mixing system is to simultaneously maintain the delivery pressure and
 51           mixing ratio by providing whatever total flow rate of gas (between
 52           zero and 5.28 standard liters per minute [SLM]) is demanded by the
 53           detectors.  This is accomplished by controlling two flow valves (argon
 54           and ethane) so that they each flow the same volume of gas while
 55           keeping the output pressure nearly constant. The mixing system flow
 56           diagram is shown in Fig. \ref{fig:gas_mixer_diagram}.
 57           %=====================================================================
 58 saw   1.5 %=====================================================================
 59 saw   1.2 \section{Gas Interlock System}
 60 saw   1.5 The flow of gas from the supply bottles may be automatically shut off
 61           by normally-closed solenoid valves installed in the primary argon and
 62           ethane manifolds. Several conditions such as over-temperature, fan
 63           failure, gas leak, and fire alarm must all be in the non-alarm state
 64           before these valves will open. Alarm conditions are indicated on the
 65           gas system alarm panel on the lower-left side of the center
 66           counting-house console.
 67           
 68           When any of the required conditions is not satisfied the sounder on
 69           the panel in the counting room will make an annoying noise and both
 70           solenoid valves will close. The audible alarm may be silenced by a
 71           toggle switch on the panel. Be certain to return it to the ``on''
 72           position as soon as the fault is cleared.
 73           
 74           The most confusing, but most common alarm condition is ``Low
 75           Pressure''.  The solenoid valves will not remain open unless there is
 76           already ample pressure on the output side of both valves. This
 77           prevents, for example, the flow of pure ethane to the drift chambers
 78           when the argon bottle is empty. The way to clear this condition is to
 79           make sure there are no other faults and that both argon and ethane
 80           manifolds are properly pressurized and fitted with non-empty bottles;
 81 saw   1.5 then press and hold the ``override'' button on the alarm panel for
 82           several minutes. This button forces the solenoid valves to open even
 83           if there are fault conditions present. If all is well, gas will flow
 84           through the valves and clear the ``low pressure'' condition so that
 85           the button may be released.
 86 saw   1.2 
 87 jones 1.3 \begin{figure}[hbt]
 88 saw   1.5 \psfig{figure=drift_gas_system-gasmixer2007.eps,width=\textwidth,bbllx=12,bblly=12,bburx=750,bbury=590}
 89 saw   1.1 \caption{Diagram of Hall~C Gas Mixing System\label{fig:gas_mixer_diagram}}
 90 jones 1.3 \vspace{0.5cm}
 91 saw   1.1 \end{figure}
 92 saw   1.5 %=====================================================================
 93           %=====================================================================
 94 jones 1.3 \section{Operating the Mass Flow Controller.}
 95 saw   1.1 
 96 jones 1.3 The gas flow is controlled by a MKS~647 controller and mass flow
 97 saw   1.5 control valves.  Delivery pressure is sensed at the mixer output by a
 98           {\it Baratron} pressure transducer.  The 647 is menu driven from a
 99           display on the front panel using a keypad with numeric and cursor
100           controls for input. It features a non-volatile memory so that most of
101           its settings are retained even if the unit is unpowered.  The
102           pressure-regulation parameters do need to be reset if power is lost,
103           however, so the controller is powered through an uninterruptible power
104           supply (UPS).
105           
106           The temperature of the control
107           system must be maintained within the
108           operating range of the MKS~647 (15\degg C - 40\degg C), the pressure
109           transducer (0\degg C - 50\degg C), and the mass-flow meters and valves
110           (0\degg C - 50\degg C).  Therefore,
111           the heating and cooling systems in the gas shed must be maintained in
112           working order. The temperature is indicated by the
113           red LED display labeled \emph{Controller Temperature},
114           located in the right-hand rack of the gas shed.
115 jones 1.3 
116 saw   1.5 %=====================================================================
117           %=====================================================================
118 jones 1.3 \subsection{Settings for Normal Operation}
119           
120 saw   1.5 A summary of all of the settings required to make the controller
121           function properly is given in Table~\ref{tab:mixer_nominals}. The
122           table also shows which screen contains each parameter. Instructions
123           for setting parameters are given below. Detailed instructions for
124           configuring and operating the MKS~647 can be found in the
125           manufacturer's instruction manual\cite{647C_EN_0504A1}.
126           
127 jones 1.3 \begin{table}[hbt]
128           \begin{minipage}[h!]{\textwidth}
129           {\scriptsize
130 saw   1.5 \begin{center}
131 jones 1.3 \begin{tabular}{|l|c|l|}
132           \hline
133           Parameter   & Set To   & {\it Controller Screen}/Comments\\ \hline
134           \multicolumn{2}{|c|}{\bf Manual Valves  } &  Valves are labeled        \\
135           Valves 1, 2, 4, 8 & OPEN                  &         \\
136           Valves 3, 5, 6, 7 & CLOSED                &         \\ \hline
137 saw   1.5 \multicolumn{2}{|c|}{\bf Pressure PID Loop Settings   } & {\it Pressure Control} (Fig. \ref{fig:pressure_control})  \\
138 jones 1.3 Pressure    & 500 Torr &                   \\
139           PID Mode    & AUTO     &                   \\
140           PID GAIN    & 4.0      &                   \\
141           PID INTEG   & 10.0     &                   \\
142           PID LEAD    & 0.000    &                   \\ \hline
143 saw   1.5 \bf Mixture     & 1        & {\it User} (Fig. \ref{fig:user_display})/ Lower-right corner\\ \hline
144           \multicolumn{2}{|c|}{\bf Gas Composition for Mixture 1} & {\it Gas Composition} (Fig. \ref{fig:gas_composition})\\
145           Channel 1   & 1.000    &  (Argon)                 \\
146           Channel 2   & 1.000    &  (Ethane)                 \\
147 jones 1.3 Channel 3   & 0.000    &                   \\
148           Channel 4   & 0.000    &                   \\ \hline
149 saw   1.5 \multicolumn{2}{|c|}{\bf MFC Valve Size } & {\it Range Selection} (Fig. \ref{fig:range_selection})  \\
150           \multicolumn{2}{|c|}{\bf  / Gas}             & {\it Gas Selection} (Fig. \ref{fig:gas_selection})  \\
151           Channel 1   & 2.0 SLM / Ar         & provides 2.78 SLM Argon\\
152           Channel 2   & 5.0 SLM / C$_2$H$_6$ & provides 2.50 SLM Ethane\\
153 jones 1.3 Channel 3   & \it unused&                  \\
154           Channel 4   & \it unused&                  \\ \hline
155 saw   1.5 \multicolumn{2}{|c|}{\bf Channels ON/OFF Settings} & {\it Extended Display} (Fig. \ref{fig:extended_display})   \\
156 jones 1.3 Channel 1   & ON       &                   Press ``ON 1'' (\em Argon)  \\
157           Channel 2   & ON       &                   Press ``ON 2'' (\em Ethane) \\
158           Channel 3   & OFF      &                   Press ``OFF 3'' (\em not in use) \\
159           Channel 4   & OFF      &                   Press ``OFF 4'' (\em not in use) \\ \hline
160 saw   1.5 \multicolumn{2}{|c|}{\bf Pressure Transducer} & {\it Pressure Setup}  \\
161           Controller  & STD      &                   \\ 
162           Range F.S.  & 1000 Torr&                   \\ \hline
163           \multicolumn{2}{|c|}{\bf MFC Valve Controls     } & {\it Mode Selection} (Fig. \ref{fig:mode_selection}) \\
164 jones 1.3 Channel 1   & PID      &                                   \\
165           Channel 2   & SLAVE / 1&                                   \\
166           Channel 3   & INDEP    &                                   \\
167           Channel 4   & INDEP    &                                   \\ \hline
168           \bf Alcohol Temp. & $2^\circ $ C & Electronic Temperature  \\
169                             &              & Control Box             \\ \hline
170           \hline
171           \end{tabular}
172 saw   1.5 \end{center}
173           }%end of \scriptsize
174 jones 1.3 \end{minipage}
175           \caption{Normal Valve and Parameter Settings for the Gas Mixing System.
176           \label{tab:mixer_nominals}}
177           \end{table}
178 saw   1.5 %=====================================================================
179           \subsection{General Operation of the Mass Flow Controller}
180           If the controller screen is dark, press {\bf ESC} to awaken the
181           display.  Many screens merely provide a menu of other screens you may
182           access: simply press the item number you desire. To go up one level in
183           the menu hierarchy, press {\bf ESC}. The \emph{Menu Tree} for the 647C
184           controller is shown in Fig. \ref{fig:command_tree}.
185           
186           In general, to change a parameter displayed on the controller screen
187           use the {\bf left/right} arrow keys to move the cursor to the item you
188           wish to change. Then either use the number keys to enter the value
189           desired for that item (numeric parameter) or use the {\bf ENTER} or
190           {\bf up/down} keys to cycle a parameter through its available settings
191           (configuration parameter). Numeric parameters may be incrementally
192           modified by using the {\bf up/down} arrow keys. To make certain that a
193           new parameter becomes active, move the cursor off of the parameter
194           after you have entered the new value.
195           
196           The initial menu upon startup is the {\bf Main Menu}
197           (Fig.~\ref{fig:main_menu}).  For normal operation use the {\bf User
198           Display} menu (Fig.~\ref{fig:user_display}). It shows the amount of
199 saw   1.5 each gas currently flowing, the total gas flow, and the current
200           delivery pressure. This display also shows which of several possible
201           pre-defined gas mixtures is selected. These mixtures are configured 
202           on the {\bf Gas Composition} screen, Fig. \ref{fig:gas_composition}.
203           For normal operation, we use
204           only mixture {\bf \#1}, (number shown on the lower-right of the
205           display). {\bf Only on this screen can this parameter be changed.}
206           Mixture {\bf \#2} is usually configured to provide 100\% argon for
207           purging flammable gas out of the chambers.
208           
209           The {\bf Extended Display} menu (Fig.~\ref{fig:extended_display})
210           shows actual flow, flow set point, units, valve full-scale range, gas
211           calibration factor, whether that channel is enabled, and whether each
212           channel is operating in master, slave, PID, or independent mode. This
213           display is most useful to a system expert wishing to verify the system
214           parameter settings.  Most parameters cannot be modified from this
215           screen, however.
216           
217           Delivery pressure set-point and pressure \emph{PID-loop} control parameters
218           may be configured from the {\bf Pressure Control} screen
219           (Fig.~\ref{fig:pressure_control}).
220 saw   1.5 %
221           \begin{figure}[tb]
222           \begin{center}
223           \framebox{
224           \begin{minipage}{.65\textwidth}
225           \footnotesize
226           \begin{itemize}
227           \item MAIN MENU (Fig. \ref{fig:main_menu})
228              \begin{enumerate}
229              \item [1] USER DISPLAY (Fig.\ref{fig:user_display})
230              \item [2] EXTENDED DISPLAY (Fig.~\ref{fig:extended_display})
231              \item [3] PRESSURE CONTROL (Fig.~\ref{fig:pressure_control})
232              \item [4] DIAGNOSTICS
233                 \begin{enumerate}
234                 \item [4.1] ERROR LISTING
235                 \item [4.2] SIGNALS
236                 \end{enumerate}
237              \item [5] INSTRUMENT SETUP
238                 \begin{enumerate}
239                 \item [5.1] RANGE SELECTION (Fig.~\ref{fig:range_selection})
240                 \item [5.2] GAS SELECTION (Fig.~\ref{fig:gas_selection})
241 saw   1.5       \item [5.3] MODE SELECTION (Fig.~\ref{fig:mode_selection}) 
242                 \item [5.4] ZERO ADJUST
243                 \item [5.5] TRIP LIMITS
244                 \item [5.6] GAS COMPOSITION (Fig.~\ref{fig:gas_composition})
245                 \end{enumerate}
246              \item [6] SYSTEM SETUP
247              \item [7] PRESSURE SETUP 
248              \item [ ]
249              \item [9] INFORMATION
250              \item [0] POWER OFF
251              \end{enumerate}
252           \end{itemize}
253           \end{minipage}
254           } %%end of \framebox{
255           \caption{Command Tree for the MKS-647C Control Panel}
256           \label{fig:command_tree}
257           \end{center}
258           \end{figure}
259           %
260 jones 1.3 \begin{center}
261           \begin{figure}[hbt]
262           \begin{minipage}{2.7in}
263 saw   1.5 \psfig{figure=drift_gas_system-main_menu.eps,width=2.6in,height=1.8in}
264           \caption{MKS~647 Main Menu\label{fig:main_menu}}
265 jones 1.3 \end{minipage}
266           \begin{minipage}{2.7in}
267 saw   1.5 \psfig{figure=drift_gas_system-user_display.eps,width=2.6in,height=1.8in}
268           \caption{MKS~647 User Display\label{fig:user_display}}
269 jones 1.3 \end{minipage}
270           \end{figure}
271           \end{center}
272 saw   1.5 %
273 jones 1.3 \begin{center}
274           \begin{figure}[hbt]
275           \begin{minipage}{2.7in}
276 saw   1.5 \psfig{figure=drift_gas_system-extended_display.eps,width=2.6in,height=1.8in}
277 jones 1.3 \caption{Extended Display Screen\label{fig:extended_display}}
278           \end{minipage}
279           \begin{minipage}{2.7in}
280 saw   1.5 \psfig{figure=drift_gas_system-pressure_control.eps,width=2.6in,height=1.8in}
281 jones 1.3 \caption{Pressure Control Screen\label{fig:pressure_control}}
282           \end{minipage}
283           \end{figure}
284           \end{center}
285 saw   1.5 %=====================================================================
286 jones 1.3 \subsection{Gas Flow Rates}
287           \label{sec:gas_flow_rates}
288           The flow rates are adjusted automatically by the controller in order
289           to maintain a constant delivery pressure at the output. Only the flow
290 saw   1.5 {\em ratios} should be set by the operator. We use a 1:1 ratio, set on
291           the {\bf Gas Composition} screen (Fig.~\ref{fig:gas_composition}), as
292           indicated in Table~\ref{tab:mixer_nominals}.
293           
294           The average total flow should equal the sum of the flows to all of the
295           detectors in the shield house. (Note that the ball-type flowmeters in
296           the shield house are calibrated for nitrogen. The approximate
297           multiplier to convert these readings for 50/50 Argon-Ethane is 0.9 .)
298 jones 1.3 
299           System configuration parameters specifying the full-scale flow
300           capacity (for nitrogen) of each valve, the types of gases actually
301 saw   1.5 flowing through each valve, and the mode of control for the valves are
302           set in the screens pictured in Figs.~\ref{fig:range_selection},
303           \ref{fig:gas_selection}, and \ref{fig:mode_selection}. These figures
304           show the nominal settings for the Hall-C system.
305 jones 1.3 
306           \begin{center}
307           \begin{figure}[hbt]
308           \begin{minipage}{2.7in}
309 saw   1.5 \psfig{figure=drift_gas_system-gas_composition.eps,width=2.6in,height=1.8in}
310 jones 1.3 \caption{Gas Composition Screen\label{fig:gas_composition}}
311           \end{minipage}
312           \begin{minipage}{2.7in}
313 saw   1.5 \psfig{figure=drift_gas_system-range_selection.eps,width=2.6in,height=1.8in}
314 jones 1.3 \caption{Range Selection Screen\label{fig:range_selection}}
315           \end{minipage}
316           \end{figure}
317           \begin{figure}[hbt]
318           \begin{minipage}{2.7in}
319 saw   1.5 \psfig{figure=drift_gas_system-gas_selection.eps,width=2.6in,height=1.8in}
320 jones 1.3 \caption{Gas Selection Screen\label{fig:gas_selection}}
321           \end{minipage}
322           \begin{minipage}{2.7in}
323 saw   1.5 \psfig{figure=drift_gas_system-mode_selection.eps,width=2.6in,height=1.8in}
324 jones 1.3 \caption{Mode Selection Screen\label{fig:mode_selection}}
325           \end{minipage}
326           \end{figure}
327           \end{center}
328 saw   1.1 
329 saw   1.5 %=====================================================================
330 jones 1.3 \subsection{To set the Delivery Pressure:}
331 saw   1.1 
332 saw   1.5 Navigate to the {\bf Pressure Control} menu. The pressure set-point (in
333           Torr) is indicated at the bottom-center of the screen. This value
334           should be se to 500.0. Note that the system can not respond instantly
335           to a change in requested gas pressure: it has no way to release excess
336           pressure and must wait for the detector systems to consume it
337           \footnote{An \emph{over-pressure relief valve} releases gas through a
338           small oil bubbler in the gas shed if the pressure exceeds about
339           600~Torr.}; it cannot build up pressure any faster than the
340           flow-control valves can supply it. It may take thirty minutes or so
341           for the pressure regulation system to stabilize at a new set-point or
342           stabilize in response to a change in total gas consumption. However,
343           you should be able to observe a change in the gas flow within a few
344           seconds (possibly up to a minute) after a set-point change.
345 saw   1.1 
346 saw   1.5 %=====================================================================
347 saw   1.1 \subsection{To turn gas flow on or off:}
348           
349 saw   1.5 The gas flow can be turned on or off while in any menu.  In the
350           Extended Display menu the bottom line displays ``ON'' or ``OFF'', by
351           channel, to show which mass flow valves are enabled.  ``ON" must be
352           displayed in the bottom row of the Extended Display menu for gas to be
353           flowing in a particular channel.
354 saw   1.1 
355 saw   1.5 For gas to flow, two conditions must be met: 
356           \begin{enumerate}
357           \item Each channel (1 and 2) must be enabled by pressing ``ON" and then
358           the desired channel number.
359           \item The entire system must be enabled by pressing
360           ``ON" and then ``ALL" from the keypad. 
361           \end{enumerate}
362           Thus, each valve can be controlled individually using ``ON/OFF~-~\emph{Channel Number}'',
363           or all flow can be controlled using ``ON/OFF~-~ALL''. If the system
364           is enabled, the status line at the bottom of every screen will
365           indicate ``FLOW ON GAS ON''. {\bf Note:} because Valve-2 (ethane) is 
366           normally slaved to Valve-1 (argon), when Valve-1 is disabled there will
367           be no flow through Valve-2.
368           
369           %=====================================================================
370           %=====================================================================
371 saw   1.1 \section{To Change a Gas Bottle}
372           
373 saw   1.2 The argon and ethane supply bottles should be replaced by new (full)
374 saw   1.5 bottles when the bottle content drops below about 10\% of its
375           capacity.  For argon, the bottle content is directly indicated by the
376           bottle pressure: a new bottle usually contains 2000 to
377           3000~psig. Argon bottles should be changed whenever the bottle
378           pressure is found to be below about 200~psig. 
379           
380           Ethane bottles, on the
381           other hand, contain liquefied ethane. Thus the bottle pressure is just
382           the vapor pressure of ethane at whatever the current temperature
383           happens to be. At 70\degg F this is about 544~psig. The pressure gauge
384           will not tell you how much ethane is left in the bottle until it reads
385           zero! Instead, we measure the ethane content by observing the weight
386           of the bottle and comparing it to the weight when the bottle was
387           full. A standard B-size cylinder contains about 32~pounds of ethane.
388           The ethane cylinders on the manifold sit on scales which have been 
389           pre-set to indicate the net weight of ethane in the bottle.
390           Numbers in the green portion of the dial indicate ethane remaining.
391           If the indicator points to the red portion of the dial, the bottle
392           is empty.
393           
394           Handling and connecting bottles of compressed gas require special
395 saw   1.5 knowledge.  The high pressure gas stored in the cylinders (bottles)
396           constitutes significant stored energy. Mishandling of a gas bottle can
397           pose a lethal hazard! Refer to the JLab ESH\&Q Manual\cite{bi:jlabehs}
398           for safe handling practices. If you do not already know how to safely
399           manipulate compressed gas hardware, have a knowledgeable person train
400           you.
401           
402           After attaching a new gas bottle to the supply manifold, check the
403           connection for leaks using \emph{Snoop} or a similar leak detector.
404           
405           %=====================================================================
406           %=====================================================================
407           \section{The Alcohol Bubbler}
408 saw   1.1 
409 jones 1.3 To reduce the rate of aging of the wire chambers, the operating gas
410           contains a small quantity of alcohol vapor. The vapor is added by
411           bubbling the argon/ethane mixture through liquid alcohol. The
412           temperature of the alcohol controls the alcohol vapor pressure, which
413           determines the amount of vapor added to the gas. The alcohol content
414           also affects the electron drift velocity in the wire chambers, so it
415           must be held approximately constant.
416           
417 saw   1.5 Gas is bubbled through the liquid alcohol inside the glass
418           dome vessel in the refrigerator. The dome is covered by a
419           perforated steel cylinder as a precaution against breakage. The
420           alcohol level is controlled by a float valve inside the metal cold
421           reservoir, which is also inside the refrigerator. As long as there is
422           alcohol in the warm reservoir (sitting on top of the refrigerator),
423           the liquid levels inside the refrigerator will remain constant. A
424           drain valve (\#7) inside the refrigerator is available for emptying
425           all liquid from the system.  It is for use by experts only and should
426           remain closed during normal operation.
427           
428           {\bf The reservoir should be refilled before it becomes empty to
429           maintain a head of liquid over the float valve.  This will prevent air
430           from entering the system.}
431           %=====================================================================
432           \subsection{To by-pass the alcohol system}
433           
434           Open valve {\bf 3}, then promptly close valves {\bf 1 \& 2}, in that order!
435           
436           \noindent To restore flow through the bubbler, open valves {\bf 1 \& 2} then
437           close valve {\bf 3}.
438 saw   1.5 
439           %=====================================================================
440           \subsection {Alcohol Temperature Control}
441           
442           To keep the alcohol temperature (and thus the vapor pressure) constant,
443           the alcohol bubbler is housed in a refrigerator which is controlled by
444           an electronic temperature regulator having 1~C\degg  sensitivity. The 
445           controller is located on a shelf in the right-hand rack of the gas mixing
446           system. Normally, the actual temperature in the refrigerator is
447           indicated on the front panel of the controller. The controller should
448           be set to maintain a temperature of 2\degg  C.
449           
450           %=====================================================================
451           \pagebreak[4] 
452           \subsection{Step-by-Step Instructions for Refilling the Alcohol Bubbler}
453           {\em These 13 steps must be individually completed in the order listed!}
454           Refer to Fig.~\ref{fig:gas_mixer_diagram}.\\
455           
456           \begin{minipage}{\textwidth}
457 saw   1.1 \begin{enumerate}
458 saw   1.5 \footnotesize{
459 jones 1.3 \item{Remove the three screws securing the cover on the alcohol fill-tank 
460           (the top-most metal tank at the rear of the mixer rack. Carefully remove the lid
461           without allowing dust or dirt to fall into the tank.}
462           \item{Fill this tank to about 75\% full from a bottle of 2-propanol.}
463           \item{Replace the lid and retaining screws.}
464           \item{Remove the small brass cap which seals the port on the lid.}
465           \item{Isolate the warm reservoir by {\bf closing valves 4 and 8.}}
466           \item{Release pressure in the warm reservoir by {\bf slowly opening valve 6 fully.}}
467           \item{{\bf Open valve 5 fully} to begin the flow of alcohol from the fill-tank to the warm reservoir.}
468           \item{{\bf Monitor the level} of alcohol in the warm reservoir sight-tube.}
469           \item{When the level is 2~cm from the top of the sight-tube, {\bf close valve 5.}}
470           \item{Replace the brass cap on the lid of the fill-tank.}
471           \item{{\bf Close valve 6, {\it then} slowly open valve 4.}}
472           \item{{\bf Open valve 8.}}
473 saw   1.5 \item{Record what you did in both the gas logbook and the electronic logbook.}
474           } %end of scriptsize 
475 saw   1.1 \end{enumerate}
476 saw   1.5 \end{minipage}
477 saw   1.1 
478 saw   1.5 %=====================================================================
479           %=====================================================================
480 saw   1.1 \section{Gas Filters Maintenance}
481           
482           There are gas filters on the argon and ethane supply lines just inside
483           the gas shed. These filters should be replaced on a regular schedule.
484           See Bill Vulcan for details.
485           
486 saw   1.5 %=====================================================================
487           %=====================================================================
488 saw   1.1 \section{Secure Pressure Regulators}
489           
490           The gas mixing system is protected from failure or mis-setting of the 
491           primary pressure regulators (the ones mounted on the manifolds on the
492           exterior of the gas shed -- near the bottles) by {\it hidden} regulators
493           mounted just inside the gas shed. It is these regulators which actually
494           set the maximum supply pressure to the mixing valves. These regulators
495           should {\em never} be adjusted by other than a gas system expert! The
496           nominal secondary pressure supplied by both the argon and ethane
497 jones 1.3 secure regulators is 30 psig.
498           
499 saw   1.5 %=====================================================================
500           %=====================================================================
501 jones 1.3 \section{Ethane Flow Restrictor}
502           
503           A calibrated flow-restricting orifice is installed at the outlet of
504           the main ethane high-pressure manifold outside the gas shed. This
505           orifice passively limits the flow rate of ethane into the gas shed
506           even if there is a catastrophic failure of the flow and pressure-controlling
507           devices inside the shed. It is model {\tt IC-DM4-9-SS} manufactured by
508           {\em O'Keefe Controls Co.}, Trumbull, CT, USA. While it may look like
509           simply a stainless-steel union fitting, it is in fact a precision part,
510           and a necessary component of the gas safety system. It limits the flow
511 saw   1.5 of ethane to less than 26.5 SLM, which is a little
512 jones 1.3 less than ten times the maximum capacity of the flow-control system.
513 saw   1.1 
514 saw   1.5 %=====================================================================
515           %=====================================================================
516           
517           \raggedright  %this fixes formatting of bibliography, too.
518 saw   1.1 
519           \section{Related {\it Howtos}}
520           \begin{itemize}
521 jones 1.3 \item MKS~647 Mass Flow Controller Manual \cite{647C_EN_0504A1}
522 saw   1.1 \item Base Equipment Shift Checklist Items \cite{howto:base_equip_checklist}
523           \end{itemize}
524           
525           \end{document}
526           
527           % Revision history:
528           %  1st draft by Howard Fenker 27FEB03 -- taken from existing ops manual.
529 jones 1.3 %  Rev. 1.1 - added notes on bottle changing, ethane bottle pressure.
530           % $Log$

Analyzer/Replay: Mark Jones, Documents: Stephen Wood
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